Advanced Study Group Diffusion and Microstructure Analysis (DMA)
Effect of heat treatment on diffusion, internal friction, microstructure and mechanical properties of ultra-fine-grained nickel severely deformed by equal-channel angular pressing
S. V. Divinski, G. Reglitz, I. S. Golovin, M. Peterlechner, R. Lapovok, Y. Estrin, G. Wilde.
Acta Materialia, 82, 11-21, (2015)
Severe plastic deformation via equal-channel angular pressing was shown to induce characteristic ultra-fast diffusion paths in Ni (Divinski et al., 2011). The effect of heat treatment on these paths, which were found to be represented by deformation-modified general high-angle grain boundaries (GBs), is investigated by accurate radiotracer self-diffusion measurements applying the 63Ni isotope. Redistribution of free volume and segregation of residual impurities caused by the heat treatment triggers relaxation of the diffusion paths. A correlation between the GB diffusion kinetics, internal friction, microstructure evolution and microhardness changes is established and analyzed in detail. A phenomenological model of diffusion enhancement in deformation-modified GBs is proposed.